INFRARED SPECTROSCOPY

EXERCISE #1

Alkanes vs. Alkenes

These classes of compounds should be easy to distinguish by IR: alkenes will have peaks for sp2 CH’s and the C=C, while alkanes will not. However, the C=C peak for an alkene can be small and hard to find unless the alkene: a) is terminal or b) has a polarizing substituent attached to it. In rare cases, you may have a tetra-substituted alkene, in which case there will of course be no sp2 C-H peaks. For alkenes, peaks in the fingerprint region can give information about the substitution pattern.

The compounds used in this exercise are hexane and 1-hexene. See if you can figure out which one is which.

Compound A:

Expand any region:
4000 - 3200 cm-1 3200 - 2700 cm-1 2700 - 2000 cm-1 2000 - 1660 cm-1 1660 - 1400 cm-1 1400 - 900 cm-1 900 - 600 cm-1
Get the molecular formula of this compound. Get the name of this compound. Get the structure of this compound. Go to the IR data tables. Get an unknown. Go back to the IR exercise homepage.

Compound B:

Expand any region:
4000 - 3200 cm-1 3200 - 2700 cm-1 2700 - 2000 cm-1 2000 - 1660 cm-1 1660 - 1400 cm-1 1400 - 900 cm-1 900 - 600 cm-1
Get the molecular formula of this compound. Get the name of this compound. Get the structure of this compound. Go to the IR data tables. Get an unknown. Go back to the IR exercise homepage.